Information card for entry 7700793

Structure parameters

• Formula: C32 H38 Mo2 N14 O9
• Calculated formula: C32 H38 Mo2 N14 O9
• Title of publication: [3 + 2] cycloaddition of azido-bridged molybdenum(ii) complex with nitriles and alkynes.
• Authors of publication: Chen, You-Xuan; Yang, Hsueh-Hui; Lin, Yu-Liang; Hou, Ji-Kuan; Chu, Yong-Jui; Liu, Fu-Chen; Lee, Gene-Hsiang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12996 - 13005
• a: 12.354 ± 0.0006 Å
• b: 12.9495 ± 0.0007 Å
• c: 14.5236 ± 0.0007 Å
• α: 66.3975 ± 0.0012°
• β: 70.1697 ± 0.001°
• γ: 77.655 ± 0.0011°
• Cell volume: 1994.63 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1357
• Weighted residual factors for all reflections included in the refinement: 0.1451
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No