Information card for entry 7701172

Structure parameters

• Formula: C30 H34 Mo O7 P Re
• Calculated formula: C30 H34 Mo O7 P Re
• Title of publication: One-step synthesis and P-H bond cleavage reactions of the phosphanyl complex syn-[MoCp{PH(2,4,6-C₆H₂^tBu₃)}(CO)₂] to give heterometallic phosphinidene-bridged derivatives.
• Authors of publication: Alvarez, M. Angeles; Burgos, Mónica; García, M Esther; García-Vivó, Daniel; Ruiz, Miguel A.; Vega, Patricia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 39
• Pages of publication: 14585 - 14589
• a: 10.3435 ± 0.0003 Å
• b: 10.6128 ± 0.0003 Å
• c: 14.9254 ± 0.0004 Å
• α: 74.056 ± 0.003°
• β: 81.568 ± 0.003°
• γ: 82.695 ± 0.003°
• Cell volume: 1551.84 ± 0.08 ų
• Cell temperature: 149.8 ± 0.2 K
• Ambient diffraction temperature: 149.8 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0276
• Residual factor for significantly intense reflections: 0.0234
• Weighted residual factors for significantly intense reflections: 0.0621
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.126
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No