Information card for entry 7701209

Structure parameters

• Formula: C30 H51 Fe N2 O P Si4
• Calculated formula: C30 H51 Fe N2 O P Si4
• Title of publication: Magnetic anisotropy in trigonal planar Fe(ii) bis(trimethylsilyl)amido complexes of the type [Fe{N(SiMe₃)₂}₂L]-experiment and theory.
• Authors of publication: Bodenstein, Tilmann; Eichhöfer, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 41
• Pages of publication: 15699 - 15712
• a: 12.179 ± 0.002 Å
• b: 15.406 ± 0.003 Å
• c: 20.294 ± 0.004 Å
• α: 90°
• β: 96.63 ± 0.03°
• γ: 90°
• Cell volume: 3782.3 ± 1.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No