Information card for entry 7701543

Structure parameters

• Formula: C22 H62 N4 O2 Rb2 Si4
• Calculated formula: C22 H62 N4 O2 Rb2 Si4
• Title of publication: Bis(trimethylsilyl)amide complexes of s-block metals with bidentate ether and amine ligands.
• Authors of publication: Schüler, Philipp; Görls, Helmar; Westerhausen, Matthias; Krieck, Sven
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 24
• Pages of publication: 8966 - 8975
• a: 10.0974 ± 0.0003 Å
• b: 10.299 ± 0.0003 Å
• c: 10.9912 ± 0.0004 Å
• α: 72.113 ± 0.002°
• β: 65.759 ± 0.001°
• γ: 72.496 ± 0.002°
• Cell volume: 971.55 ± 0.06 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0669
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1264
• Weighted residual factors for all reflections included in the refinement: 0.1363
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No