Information card for entry 7701546

Structure parameters

• Formula: C22 H62 Cs2 N4 O2 Si4
• Calculated formula: C22 H62 Cs2 N4 O2 Si4
• Title of publication: Bis(trimethylsilyl)amide complexes of s-block metals with bidentate ether and amine ligands.
• Authors of publication: Schüler, Philipp; Görls, Helmar; Westerhausen, Matthias; Krieck, Sven
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 24
• Pages of publication: 8966 - 8975
• a: 8.6707 ± 0.0002 Å
• b: 11.8156 ± 0.0002 Å
• c: 20.4375 ± 0.0004 Å
• α: 106.144 ± 0.001°
• β: 95.431 ± 0.001°
• γ: 101.977 ± 0.001°
• Cell volume: 1941.43 ± 0.07 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0556
• Weighted residual factors for all reflections included in the refinement: 0.0578
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No