Information card for entry 7701658

Structure parameters

• Formula: Cs5.37 O65.6 Ru Sb W17
• Calculated formula: Cs5.36 O65.6 Ru Sb W17
• Title of publication: Reactions of [Ru(NO)Cl₅]^2- with pseudotrilacunary {XW₉O₃₃}^9- (X = As^III, Sb^III) anions.
• Authors of publication: Mukhacheva, Anna A.; Shmakova, Alexandra A.; Volchek, Victoria V.; Romanova, Tamara E.; Benassi, Enrico; Gushchin, Artem L.; Yanshole, Vadim; Sheven, Dmitri G.; Kompankov, Nikolay B.; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 42
• Pages of publication: 15989 - 15999
• a: 12.5497 ± 0.0004 Å
• b: 18.5385 ± 0.0007 Å
• c: 15.6808 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3648.2 ± 0.2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.155
• Weighted residual factors for all reflections included in the refinement: 0.1641
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No