Information card for entry 7702319

Structure parameters

• Formula: C28 H18 N14 Pt3 S8
• Calculated formula: C28 H18 N14 Pt3 S8
• Title of publication: Structural studies of [Pt(CNMe)4][M(mnt)2]n {M = Pd or Pt, mnt = [S2C2(CN)2]2−, n = 1 or 2}: structure-dependent paramagnetism of three crystal forms of [Pt(CNMe)4][Pt(mnt)2]2
• Authors of publication: Bois, Hugues; Connelly, Neil G.; Crossley, John G.; Guillorit, Jean-Christophe; Lewis, Gareth R.; Orpen, A. Guy; Thornton, Peter
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 17
• Pages of publication: 2833
• a: 14.071 ± 0.004 Å
• b: 14.414 ± 0.004 Å
• c: 20.747 ± 0.006 Å
• α: 90°
• β: 91.16 ± 0.02°
• γ: 90°
• Cell volume: 4207 ± 2 ų
• Cell temperature: 298 ± 5 K
• Ambient diffraction temperature: 298 ± 5 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for all reflections: 0.1268
• Weighted residual factors for significantly intense reflections: 0.1044
• Goodness-of-fit parameter for all reflections: 0.937
• Goodness-of-fit parameter for significantly intense reflections: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No