Crystallography Open Database

Information card for entry 7702376

Preview

Coordinates	7702376.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64.5 H60 B3 N12 U
Calculated formula	C64.5 H48 B3 N12 U
Title of publication	Synthesis and structure of uranium(III) complexes with dihydrobis(pyrazolyl)borates
Authors of publication	Maria, Leonor; Campello, Maria Paula; Domingos, Ângela; Santos, Isabel; Andersen, Richard
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	2015
a	13.565 ± 0.001 Å
b	15.715 ± 0.002 Å
c	15.929 ± 0.002 Å
α	118.957 ± 0.009°
β	92.65 ± 0.011°
γ	97.356 ± 0.015°
Cell volume	2923.7 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0726
Residual factor for significantly intense reflections	0.0501
Weighted residual factors for all reflections	0.1401
Weighted residual factors for significantly intense reflections	0.1161
Goodness-of-fit parameter for all reflections	1.087
Goodness-of-fit parameter for significantly intense reflections	1.102
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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