Information card for entry 7702392

Structure parameters

• Formula: C112 H248 I28 N8 Pb10
• Calculated formula: C112 H248 I28 N8 Pb10
• Title of publication: Discrete and polymeric iodoplumbates with Pb3I10 building blocks: [Pb3I10]4−, [Pb7I22]8−, [Pb10I28]8−, 1\ιnfty [Pb3I10]4− and 2∞[Pb7I18]4−
• Authors of publication: Krautscheid, Harald; Vielsack, Frieder
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 2731
• a: 22.9116 ± 0.0009 Å
• b: 22.9116 ± 0.0009 Å
• c: 18.5203 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9722.1 ± 0.7 ų
• Cell temperature: 190 ± 2 K
• Ambient diffraction temperature: 190 ± 2 K
• Number of distinct elements: 5
• Space group number: 112
• Hermann-Mauguin space group symbol: P -4 2 c
• Hall space group symbol: P -4 2c
• Residual factor for all reflections: 0.0325
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for all reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.0605
• Goodness-of-fit parameter for all reflections: 1.033
• Goodness-of-fit parameter for significantly intense reflections: 1.042
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No