Information card for entry 7702480

Structure parameters

• Formula: C75 H89 Cl2 Cu N4 O3.5 P2
• Calculated formula: C74.5 H62 Cl2 Cu N4 O3.5 P2
• Title of publication: Synthesis and characterization of bulky salen-type complexes of Co, Cu, Fe, Mn and Ni with amphiphilic solubility properties
• Authors of publication: Haikarainen, Anssi; Sipilä, Jussi; Pietikäinen, Pekka; Pajunen, Aarne; Mutikainen, Ilpo
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 7
• Pages of publication: 991
• a: 14.941 ± 0.008 Å
• b: 19.023 ± 0.008 Å
• c: 13.869 ± 0.006 Å
• α: 95.42 ± 0.05°
• β: 116.06 ± 0.05°
• γ: 88.96 ± 0.05°
• Cell volume: 3524 ± 3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.11
• Weighted residual factors for all reflections: 0.3347
• Weighted residual factors for significantly intense reflections: 0.308
• Weighted residual factors for all reflections included in the refinement: 0.3347
• Goodness-of-fit parameter for all reflections: 1.336
• Goodness-of-fit parameter for all reflections included in the refinement: 1.336
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No