Crystallography Open Database

Information card for entry 7702515

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Coordinates	7702515.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	99002
Formula	C41 H80 O12 Si8
Calculated formula	C40.994 H60.5 O12 Si8
Title of publication	A functional model for lanthanide doped silicate materials: synthesis of an apically substituted samarium silsesquioxane complex
Authors of publication	Arnold, Polly L.; Blake, Alexander J.; Hall, Sarah N.; Ward, Benjamin D.; Wilson, Claire
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	4
Pages of publication	488
a	22.0658 ± 0.001 Å
b	17.1093 ± 0.0008 Å
c	29.2595 ± 0.0009 Å
α	90°
β	105.651 ± 0.002°
γ	90°
Cell volume	10636.8 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.173
Residual factor for significantly intense reflections	0.0758
Weighted residual factors for significantly intense reflections	0.169
Weighted residual factors for all reflections included in the refinement	0.2153
Goodness-of-fit parameter for all reflections included in the refinement	0.969
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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