Information card for entry 7702578

Structure parameters

• Formula: C6 H20 Cl4 N3 Ta
• Calculated formula: C6 H20 Cl4 N3 Ta
• Title of publication: The isolation and chemistry of niobium and tantalum dimethylamides containing mono- and di-aryloxide ancillary ligands
• Authors of publication: Schweiger, Scott W.; Tillison, Dana L.; Thorn, Matt G.; Fanwick, Phillip E.; Rothwell, Ian P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 16
• Pages of publication: 2401
• a: 8.6567 ± 0.0003 Å
• b: 17.9638 ± 0.0007 Å
• c: 10.2052 ± 0.0003 Å
• α: 90°
• β: 107.121 ± 0.002°
• γ: 90°
• Cell volume: 1516.66 ± 0.09 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for all reflections included in the refinement: 0.107
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No