Information card for entry 7702655

Structure parameters

• Formula: C24 H28 Cl N7 O7
• Calculated formula: C24 H25 Cl N7 O7
• Title of publication: Synthesis and characterisation of zinc(ii) complexes of tripodal N7 ligands involving pyridine and amine or amide nitrogen donors. Crystal structure of a zinc(ii) complex
• Authors of publication: Mohamadou, Aminou; Gérard, Christian
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 22
• Pages of publication: 3320
• a: 7.3724 ± 0.0001 Å
• b: 27.1686 ± 0.0006 Å
• c: 13.3039 ± 0.0003 Å
• α: 90°
• β: 100.696 ± 0.005°
• γ: 90°
• Cell volume: 2618.44 ± 0.1 ų
• Cell temperature: 294 K
• Ambient diffraction temperature: 294 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.123
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for all reflections: 0.203
• Weighted residual factors for all reflections included in the refinement: 0.07
• Goodness-of-fit parameter for all reflections: 3.124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No