Information card for entry 7702715

Structure parameters

• Chemical name: μ-hydrido-μ-thiolato-bis-ax-triphenylphospine- hexacarbonyl-dirhenium
• Formula: C42 H32 O6 P2 Re2 S
• Calculated formula: C42 H31 O6 P2 Re2 S
• Title of publication: Substitution reactivity of the hydrido sulfido bridged dirhenium complex [Re2(µ-H)(µ-Snaph)(CO)8] (naph = 2-naphthyl)
• Authors of publication: Egold, Hans; Schwarze, Detlef; Flörke, Ulrich
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1078
• a: 10.615 ± 0.001 Å
• b: 10.683 ± 0.001 Å
• c: 19.747 ± 0.002 Å
• α: 75.86 ± 0.01°
• β: 78.98 ± 0.01°
• γ: 68.87 ± 0.01°
• Cell volume: 2012.3 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No