Information card for entry 7702723

Structure parameters

• Formula: C37 H66 Cl O P2 Rh
• Calculated formula: C37 H66 Cl O P2 Rh
• Title of publication: Highly electron rich alkyl- and dialkyl-N-pyrrolidinyl phosphines: an evaluation of their electronic and structural properties
• Authors of publication: Clarke, Matthew L.; Holliday, Gemma L.; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1093
• a: 9.9574 ± 0.0001 Å
• b: 10.2575 ± 0.0001 Å
• c: 10.8125 ± 0.0001 Å
• α: 113.782 ± 0.001°
• β: 109.177 ± 0.001°
• γ: 90.819 ± 0.001°
• Cell volume: 940.65 ± 0.02 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0305
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.0582
• Weighted residual factors for all reflections included in the refinement: 0.0605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No