Information card for entry 7702758

Structure parameters

• Formula: C55 H95 Cs2 Li N6 O20
• Calculated formula: C55 H95 Cs2 Li N6 O20
• Title of publication: Formation of [M(15-crown-5)2]2[Li(NHPy)3] (M = K or Cs): the first structurally authenticated examples of a monomeric lithium species coordinated by three amide anions
• Authors of publication: Liddle, Stephen T.; Clegg, William
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 24
• Pages of publication: 3549
• a: 14.2706 ± 0.0009 Å
• b: 14.6824 ± 0.0009 Å
• c: 18.2599 ± 0.0011 Å
• α: 77.781 ± 0.002°
• β: 71.818 ± 0.002°
• γ: 68.921 ± 0.002°
• Cell volume: 3370.3 ± 0.4 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1194
• Residual factor for significantly intense reflections: 0.0651
• Weighted residual factors for significantly intense reflections: 0.182
• Weighted residual factors for all reflections included in the refinement: 0.2108
• Goodness-of-fit parameter for all reflections included in the refinement: 0.884
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No