Information card for entry 7702823

Structure parameters

• Formula: C4 H14 Cl2 N O8 Sm
• Calculated formula: C4 H14 Cl2 N O8 Sm
• Title of publication: Sm(iii) Complexation with amino acids. Crystal structures of [Sm2(Pro)6(H2O)6](ClO4)6and [Sm(Asp)(H2O)4]Cl2
• Authors of publication: Torres, Julia; Kremer, Carlos; Kremer, Eduardo; Pardo, Helena; Suescun, Leopoldo; Mombrú, Álvaro; Domínguez, Sixto; Mederos, Alfredo; Herbst-Irmer, Regine; Arrieta, Juan M.
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 4035
• a: 9.1372 ± 0.0018 Å
• b: 7.6379 ± 0.0015 Å
• c: 9.2014 ± 0.0018 Å
• α: 90°
• β: 91.57 ± 0.03°
• γ: 90°
• Cell volume: 641.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0357
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections included in the refinement: 0.0891
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No