Information card for entry 7702836

Structure parameters

• Chemical name: catena-oxalate-bis[1-(aminoethyl)pyrrolidine-copper(II)]- 0.5(squarate) perchlorate hydrated
• Formula: C16 H28.5 Cl Cu2 N4 O10.25
• Calculated formula: C16 H28 Cl Cu2 N4 O10.25
• Title of publication: Synthesis, crystal structure and magneto-structural correlation of two bi-bridging 1D copper(ii) chainsElectronic supplementary information (ESI) available: magnetization curve for 1 between 0 and 5 K and an EPR spectrum for 1. See http://www.rsc.org/suppdata/dt/b2/b204728b/
• Authors of publication: Mukherjee, Partha Sarathi; Konar, Sanjit; Zangrando, Ennio; Diaz, Carmen; Ribas, Joan; Ray Chaudhuri*, Nirmalendu
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 18
• Pages of publication: 3471
• a: 6.081 ± 0.003 Å
• b: 13.402 ± 0.004 Å
• c: 16.185 ± 0.005 Å
• α: 65.85 ± 0.03°
• β: 91.23 ± 0.03°
• γ: 82.25 ± 0.03°
• Cell volume: 1188.3 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0827
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1581
• Weighted residual factors for all reflections included in the refinement: 0.1725
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: mokα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No