Crystallography Open Database

Information card for entry 7703520

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Coordinates	7703520.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H37 Cl N2 O6.75 Pd2
Calculated formula	C39 H37 Cl N2 O6.75 Pd2
Title of publication	Open clamshell dinuclear palladium(ii) complexes possessing out-of-plane anisotropy.
Authors of publication	Yamamoto, Koji; Higuchi, Kazuki; Kuwata, Shigeki; Hayashi, Yoshihiro; Kawauchi, Susumu; Takata, Toshikazu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	9
Pages of publication	2781 - 2785
a	12.641 ± 0.003 Å
b	13.964 ± 0.003 Å
c	21.656 ± 0.005 Å
α	73.184 ± 0.011°
β	76.622 ± 0.012°
γ	74.112 ± 0.012°
Cell volume	3471 ± 1.4 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0794
Residual factor for significantly intense reflections	0.0557
Weighted residual factors for significantly intense reflections	0.1315
Weighted residual factors for all reflections included in the refinement	0.1407
Goodness-of-fit parameter for all reflections included in the refinement	0.807
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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