Information card for entry 7704017

Structure parameters

• Formula: C23 H8 Al Cs F36 O4
• Calculated formula: C22.9999 H8 Al Cs0.99995 F35.9998 O3.99998
• Title of publication: Building blocks for the chemistry of perfluorinated alkoxyaluminates [Al{OC(CF₃)₃}₄]^-: simplified preparation and characterization of Li⁺-Cs⁺, Ag⁺, NH₄⁺, N₂H₅⁺ and N₂H₇⁺ salts.
• Authors of publication: Malinowski, Przemysław J; Jaroń, Tomasz; Domańska, Małgorzata; Slattery, John M.; Schmitt, Manuel; Krossing, Ingo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 23
• Pages of publication: 7766 - 7773
• a: 21.7362 ± 0.0002 Å
• b: 31.2247 ± 0.0002 Å
• c: 33.096 ± 0.0003 Å
• α: 90°
• β: 107.891 ± 0.001°
• γ: 90°
• Cell volume: 21376.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1468
• Weighted residual factors for all reflections included in the refinement: 0.1541
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No