Synthesis, structural characterization and electrochemical and magnetic studies of M(hfac)<sub>2</sub> (M = Cu<sup>II</sup>, Co<sup>II</sup>) and Nd(hfac)<sub>3</sub> complexes of 4-amino-TEMPO.
Authors of publication
Navarro, Yolanda; Guedes, Guilherme P.; Cano, Joan; Ocón, Pilar; Iglesias, María José; Lloret, Francisco; López-Ortiz, Fernando
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2020
Journal volume
49
Journal issue
19
Pages of publication
6280 - 6294
a
20.826 ± 0.002 Å
b
21.226 ± 0.002 Å
c
12.0638 ± 0.0012 Å
α
90°
β
99.785 ± 0.003°
γ
90°
Cell volume
5255.3 ± 0.9 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.1008
Residual factor for significantly intense reflections
0.081
Weighted residual factors for significantly intense reflections
0.2203
Weighted residual factors for all reflections included in the refinement
0.2403
Goodness-of-fit parameter for all reflections included in the refinement
