Information card for entry 7704347

Structure parameters

• Formula: C80 H114 N2 O2 P2 Zr
• Calculated formula: C62 H72 N2 O2 P2 Zr
• Title of publication: Phosphasalen group IV metal complexes: synthesis, characterization and ring opening polymerization of lactide.
• Authors of publication: Normand, Adrien T.; Malacea-Kabbara, Raluca; Lapenta, Rosita; Dajnak, Aymeric; Richard, Philippe; Cattey, Hélène; Bolley, Anaëlle; Grassi, Alfonso; Milione, Stefano; Auffrant, Audrey; Dagorne, Samuel; Le Gendre, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 6989 - 7004
• a: 13.2872 ± 0.0007 Å
• b: 16.4819 ± 0.001 Å
• c: 16.7752 ± 0.0009 Å
• α: 69.077 ± 0.002°
• β: 75.579 ± 0.003°
• γ: 80.202 ± 0.003°
• Cell volume: 3310 ± 0.3 ų
• Cell temperature: 115 K
• Ambient diffraction temperature: 115 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0913
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1366
• Weighted residual factors for all reflections included in the refinement: 0.1546
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No