Information card for entry 7704351

Structure parameters

• Formula: C62.79 H77.45 Br0.04 N2 O2 P2
• Calculated formula: C62.788 H77.4488 Br0.0424 N2 O2 P2
• Title of publication: Phosphasalen group IV metal complexes: synthesis, characterization and ring opening polymerization of lactide.
• Authors of publication: Normand, Adrien T.; Malacea-Kabbara, Raluca; Lapenta, Rosita; Dajnak, Aymeric; Richard, Philippe; Cattey, Hélène; Bolley, Anaëlle; Grassi, Alfonso; Milione, Stefano; Auffrant, Audrey; Dagorne, Samuel; Le Gendre, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 6989 - 7004
• a: 9.628 Å
• b: 15.392 Å
• c: 19.387 Å
• α: 73.03°
• β: 82.93°
• γ: 88.87°
• Cell volume: 2726.65 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0553
• Weighted residual factors for significantly intense reflections: 0.1364
• Weighted residual factors for all reflections included in the refinement: 0.1467
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No