Information card for entry 7704361

Structure parameters

• Formula: C32 H51 B Cl2 F4 O2 P2 Ru
• Calculated formula: C32 H51 B Cl2 F4 O2 P2 Ru
• Title of publication: Conformation controlled stepwise hydride shuffling from the metal to the ligand backbone.
• Authors of publication: Wiedmaier, Nicholas R.; Speth, Hansjörg; Leistikow, Georg; Eichele, Klaus; Schubert, Hartmut; Mayer, Hermann A.; Wesemann, Lars
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 7218 - 7227
• a: 11.911 ± 0.0003 Å
• b: 12.8598 ± 0.0003 Å
• c: 23.657 ± 0.0005 Å
• α: 90°
• β: 98.835 ± 0.001°
• γ: 90°
• Cell volume: 3580.62 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.0775
• Goodness-of-fit parameter for all reflections included in the refinement: 1.253
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No