Information card for entry 7704379

Structure parameters

• Formula: C139 H172 Fe3 N8 O11 Sm2
• Calculated formula: C139 H172 Fe3 N8 O11 Sm2
• Title of publication: 3d-4f heterometallic complexes by the reduction of transition metal carbonyls with bulky Ln^II amidinates.
• Authors of publication: Yadav, Ravi; Hossain, Md Elius; Peedika Paramban, Ramees; Simler, Thomas; Schoo, Christoph; Wang, Jun; Deacon, Glen B.; Junk, Peter C.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 23
• Pages of publication: 7701 - 7707
• a: 17.4276 ± 0.0004 Å
• b: 20.8564 ± 0.0003 Å
• c: 18.053 ± 0.0004 Å
• α: 90°
• β: 93.692 ± 0.002°
• γ: 90°
• Cell volume: 6548.2 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0942
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No