Information card for entry 7704382

Structure parameters

• Formula: C63 H37 B F26 N5 Rh
• Calculated formula: C63 H37 B F26 N5 Rh
• Title of publication: Isolation and structural characterisation of rhodium(iii) η²-fluoroarene complexes: experimental verification of predicted regioselectivity.
• Authors of publication: Gyton, Matthew R.; Kynman, Amy E.; Leforestier, Baptiste; Gallo, Angelo; Lewandowski, Józef R; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 18
• Pages of publication: 5791 - 5793
• a: 12.68561 ± 0.00011 Å
• b: 27.25348 ± 0.00015 Å
• c: 18.40461 ± 0.00013 Å
• α: 90°
• β: 106.875 ± 0.0008°
• γ: 90°
• Cell volume: 6088.98 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1207
• Weighted residual factors for all reflections included in the refinement: 0.1234
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No