Information card for entry 7704399

Structure parameters

• Formula: C24 H32 F18 Fe2 Ni O21
• Calculated formula: C24 H32 F18 Fe2.001 Ni0.999 O21
• Title of publication: Heterometallic trinuclear oxo-centered clusters as single-source precursors for synthesis of stoichiometric monodisperse transition metal ferrite nanocrystals.
• Authors of publication: Sanchez-Lievanos, Karla R; Tariq, Mehrin; Brennessel, William W.; Knowles, Kathryn E.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 45
• Pages of publication: 16348 - 16358
• a: 10.5655 ± 0.0001 Å
• b: 11.5802 ± 0.0002 Å
• c: 19.9032 ± 0.0001 Å
• α: 92.634 ± 0.001°
• β: 97.241 ± 0.001°
• γ: 111.913 ± 0.001°
• Cell volume: 2229.74 ± 0.05 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0571
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for significantly intense reflections: 0.1404
• Weighted residual factors for all reflections included in the refinement: 0.1444
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No