Information card for entry 7704713

Structure parameters

• Formula: C59 H42 Al F36 Ge N2 O4 P
• Calculated formula: C59 H42 Al F36 Ge N2 O4 P
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 28.6853 ± 0.0007 Å
• b: 18.4131 ± 0.0003 Å
• c: 29.1049 ± 0.0008 Å
• α: 90°
• β: 120.236 ± 0.004°
• γ: 90°
• Cell volume: 13281.4 ± 0.8 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0901
• Residual factor for significantly intense reflections: 0.0669
• Weighted residual factors for significantly intense reflections: 0.1765
• Weighted residual factors for all reflections included in the refinement: 0.1958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No