Information card for entry 7704740

Structure parameters

• Formula: C101 H130 Dy N11 O17 Zn3
• Calculated formula: C102 H129 Dy N12 O15 Zn3
• Title of publication: Self-assembly of tetranuclear 3d-4f helicates as highly efficient catalysts for CO₂ cycloaddition reactions under mild conditions.
• Authors of publication: Yang, Huan; Gao, Guoshu; Chen, Wanmin; Wang, Li; Liu, Weisheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 29
• Pages of publication: 10270 - 10277
• a: 15.201 ± 0.0006 Å
• b: 19.7221 ± 0.0004 Å
• c: 19.7307 ± 0.0005 Å
• α: 70.729 ± 0.002°
• β: 87.962 ± 0.003°
• γ: 85.124 ± 0.002°
• Cell volume: 5563.4 ± 0.3 ų
• Cell temperature: 292 ± 2 K
• Ambient diffraction temperature: 291.73 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1031
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1377
• Weighted residual factors for all reflections included in the refinement: 0.1633
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No