Information card for entry 7705159

Structure parameters

• Formula: C30 H46 Cl4 Fe N4 Si2
• Calculated formula: C30 H46 Cl4 Fe N4 Si2
• SMILES: [Fe](Cl)(Cl)([Si]1(Cl)[N](=C(N1C(C)(C)C)c1ccccc1)C(C)(C)C)[Si]1(Cl)[N](=C(N1C(C)(C)C)c1ccccc1)C(C)(C)C
• Title of publication: Aminolysis of bis[bis(trimethylsilyl)amido]-manganese, -iron, and -cobalt for the synthesis of mono- and bis-silylene complexes.
• Authors of publication: He, Zhiyuan; Xue, Xiaolian; Liu, Yilan; Yu, Na; Krogman, Jeremy P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 36
• Pages of publication: 12586 - 12591
• a: 11.4312 ± 0.0007 Å
• b: 17.2983 ± 0.0012 Å
• c: 19.8767 ± 0.0016 Å
• α: 90°
• β: 105.599 ± 0.002°
• γ: 90°
• Cell volume: 3785.7 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1535
• Weighted residual factors for all reflections included in the refinement: 0.1709
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No