Information card for entry 7705161

Structure parameters

• Formula: C42 H82 Cl4 Fe2 N6 Si6
• Calculated formula: C42 H82 Cl4 Fe2 N6 Si6
• Title of publication: Aminolysis of bis[bis(trimethylsilyl)amido]-manganese, -iron, and -cobalt for the synthesis of mono- and bis-silylene complexes.
• Authors of publication: He, Zhiyuan; Xue, Xiaolian; Liu, Yilan; Yu, Na; Krogman, Jeremy P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 36
• Pages of publication: 12586 - 12591
• a: 10.0727 ± 0.0009 Å
• b: 12.8695 ± 0.0012 Å
• c: 13.2383 ± 0.0011 Å
• α: 67.489 ± 0.004°
• β: 85.051 ± 0.005°
• γ: 67.086 ± 0.004°
• Cell volume: 1456.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 149.99 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0994
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1199
• Weighted residual factors for all reflections included in the refinement: 0.1393
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No