Information card for entry 7705361

Structure parameters

• Formula: C55 H95 Cl N2 O2 P2 Si Ti
• Calculated formula: C55 H95 Cl N2 O2 P2 Si Ti
• Title of publication: Synthesis of compounds with C-P-P and C[double bond, length as m-dash]P-P bond systems based on the phospha-Wittig reaction.
• Authors of publication: Ziółkowska, Aleksandra; Szynkiewicz, Natalia; Pikies, Jerzy; Ponikiewski, Łukasz
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13635 - 13646
• a: 9.9454 ± 0.0004 Å
• b: 10.32 ± 0.0005 Å
• c: 27.9616 ± 0.001 Å
• α: 100.356 ± 0.003°
• β: 91.107 ± 0.003°
• γ: 95.68 ± 0.003°
• Cell volume: 2807.2 ± 0.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1363
• Residual factor for significantly intense reflections: 0.0963
• Weighted residual factors for significantly intense reflections: 0.2533
• Weighted residual factors for all reflections included in the refinement: 0.2881
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No