Information card for entry 7705482

Structure parameters

• Formula: C32.5 H42 Cl F6 N4 O1.5 Os Sb
• Calculated formula: C31 H36 Cl F6 N4 Os Sb
• Title of publication: Half-sandwich complexes of osmium containing guanidine-derived ligands.
• Authors of publication: Parker, Amie; Lamata, Pilar; Viguri, Fernando; Rodríguez, Ricardo; López, José A; Lahoz, Fernando J.; García-Orduña, Pilar; Carmona, Daniel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13601 - 13617
• a: 10.8413 ± 0.0006 Å
• b: 11.1473 ± 0.0006 Å
• c: 15.2059 ± 0.0006 Å
• α: 92.185 ± 0.001°
• β: 93.798 ± 0.001°
• γ: 110.543 ± 0.001°
• Cell volume: 1713.31 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0358
• Residual factor for significantly intense reflections: 0.0287
• Weighted residual factors for significantly intense reflections: 0.0599
• Weighted residual factors for all reflections included in the refinement: 0.0633
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No