Information card for entry 7705487

Structure parameters

• Formula: C39 H44 Cl F6 N3 Os P Sb
• Calculated formula: C39 H44 Cl F6 N3 Os P Sb
• SMILES: [Os]123456([P](CC[N]1=C(Nc1ccc(cc1)C)Nc1ccc(cc1)C)(c1ccccc1)c1ccccc1)(Cl)[c]1([cH]2[cH]3[c]4([cH]5[cH]61)C(C)C)C.[Sb](F)(F)(F)(F)(F)[F-]
• Title of publication: Half-sandwich complexes of osmium containing guanidine-derived ligands.
• Authors of publication: Parker, Amie; Lamata, Pilar; Viguri, Fernando; Rodríguez, Ricardo; López, José A; Lahoz, Fernando J.; García-Orduña, Pilar; Carmona, Daniel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13601 - 13617
• a: 10.9424 ± 0.0004 Å
• b: 13.4216 ± 0.0005 Å
• c: 25.9506 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3811.2 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0179
• Residual factor for significantly intense reflections: 0.0175
• Weighted residual factors for significantly intense reflections: 0.0409
• Weighted residual factors for all reflections included in the refinement: 0.0411
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No