Information card for entry 7705571

Structure parameters

• Formula: C39 H42 F36 K2 O16 Sn
• Calculated formula: C39 H42 F36 K2 O16 Sn
• Title of publication: Formation of monomeric Sn(ii) and Sn(iv) perfluoropinacolate complexes and their characterization by ¹¹⁹Sn Mössbauer and ¹¹⁹Sn NMR spectroscopies.
• Authors of publication: Elinburg, Jessica K.; Hyre, Ariel S.; McNeely, James; Alam, Todd M.; Klenner, Steffen; Pöttgen, Rainer; Rheingold, Arnold L.; Doerrer, Linda H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13773 - 13785
• a: 15.1378 ± 0.0016 Å
• b: 16.2438 ± 0.0016 Å
• c: 16.2454 ± 0.0016 Å
• α: 99.54 ± 0.003°
• β: 114.932 ± 0.003°
• γ: 112.822 ± 0.003°
• Cell volume: 3068.9 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.1045
• Weighted residual factors for all reflections included in the refinement: 0.1102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No