Information card for entry 7705769

Structure parameters

• Formula: C15 H23 B N O3 Si V
• Calculated formula: C15 H23 B N O3 Si V
• SMILES: [V]1234(C#[O])(C#[O])(C#[O])(=BN(C(C)(C)C)[Si](C)(C)C)[cH]5[cH]3[cH]4[cH]1[cH]25
• Title of publication: Intermetallic transfer of unsymmetrical borylene fragments: isolation of the second early-transition-metal terminal borylene complex and other rare species.
• Authors of publication: Macha, Bret B.; Dhara, Debabrata; Radacki, Krzysztof; Dewhurst, Rian D.; Braunschweig, Holger
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 48
• Pages of publication: 17719 - 17724
• a: 13.38 ± 0.005 Å
• b: 13.438 ± 0.005 Å
• c: 19.996 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3595 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.06
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No