Crystallography Open Database

Information card for entry 7705856

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Coordinates	7705856.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C130 H142 B2 F48 N2 P4 Rh2
Calculated formula	C130 H142 B2 F48 N2 P4 Rh2
Title of publication	Reactions of Rh(PNP) pincer complexes with terminal alkynes: homocoupling through a ring or not at all.
Authors of publication	Hood, Thomas M.; Chaplin, Adrian B.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	46
Pages of publication	16649 - 16652
a	23.8941 ± 0.0005 Å
b	16.1966 ± 0.0004 Å
c	37.3543 ± 0.0008 Å
α	90°
β	112.179 ± 0.003°
γ	90°
Cell volume	13386.6 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.1978
Residual factor for significantly intense reflections	0.1755
Weighted residual factors for significantly intense reflections	0.3729
Weighted residual factors for all reflections included in the refinement	0.3884
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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