Information card for entry 7706032

Structure parameters

• Formula: C82.5 H85 Dy4 N6 O29.5 P6
• Calculated formula: C80 H69 Dy4 N6 O24 P6
• Title of publication: Ring-forming transformation associated with hydrazone changes of hexadecanuclear dysprosium phosphonates.
• Authors of publication: Tian, Haiquan; Huang, Fu-Ping; Li, Yongfei; Chen, Peiqiong; Chai, Keyu; Lu, Jing; Liu, Hou-Ting; Zeng, Suyuan; Li, Dacheng; Dou, Jianmin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 3
• Pages of publication: 1119 - 1125
• a: 32.1017 ± 0.0003 Å
• b: 32.1017 ± 0.0003 Å
• c: 19.7408 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 20343.3 ± 0.5 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1498
• Weighted residual factors for all reflections included in the refinement: 0.2169
• Goodness-of-fit parameter for all reflections included in the refinement: 0.876
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No