Information card for entry 7706181

Structure parameters

• Formula: C33.94 H32 N4 O4 U
• Calculated formula: C34 H32 N4 O4 U
• Title of publication: Systematic comparison of the structure of homoleptic tetradentate N₂O₂-type Schiff base complexes of tetravalent f-elements (M(IV) = Ce, Th, U, Np, and Pu) in solid state and in solution.
• Authors of publication: Radoske, Thomas; Kloditz, Roger; Fichter, Sebastian; März, Juliane; Kaden, Peter; Patzschke, Michael; Schmidt, Moritz; Stumpf, Thorsten; Walter, Olaf; Ikeda-Ohno, Atsushi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 48
• Pages of publication: 17559 - 17570
• a: 14.6015 ± 0.0007 Å
• b: 14.6038 ± 0.0008 Å
• c: 13.9168 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2967.6 ± 0.3 ų
• Cell temperature: 106 ± 2 K
• Ambient diffraction temperature: 105.87 K
• Number of distinct elements: 5
• Space group number: 50
• Hermann-Mauguin space group symbol: P b a n :2
• Hall space group symbol: -P 2ab 2b
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0251
• Weighted residual factors for significantly intense reflections: 0.048
• Weighted residual factors for all reflections included in the refinement: 0.0547
• Goodness-of-fit parameter for all reflections included in the refinement: 1.243
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No