Information card for entry 7706757

Structure parameters

• Formula: C108 H186 N3 O37 P Si3 W9
• Calculated formula: C108 H186 N3 O37 P Si3 W9
• Title of publication: Development of sterically hindered siloxide-functionalized polyoxotungstates for the complexation of 5d-metals.
• Authors of publication: Auvray, Thomas; Nachtigall, Olaf; Brennessel, William W.; Jones, William D.; Matson, Ellen M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 12
• Pages of publication: 4300 - 4310
• a: 30.2815 ± 0.0002 Å
• b: 31.4764 ± 0.0002 Å
• c: 28.51028 ± 0.00019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 27174.6 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1356
• Weighted residual factors for all reflections included in the refinement: 0.1402
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No