Information card for entry 7706848

Structure parameters

• Common name: (5r,10s)-4-fluoro-10H-5,10-[1,2]benzenoacridophosphine
• Chemical name: (5r,10s)-4-fluoro-10H-5,10-[1,2]benzenoacridophosphine
• Formula: C19 H12 F P
• Calculated formula: C19 H12 F P
• Title of publication: Sterically hindered ortho-substituted phosphatriptycenes as configurationally stable P-chirogenic triarylphosphines.
• Authors of publication: Hu, Lei; Mahaut, Damien; Tumanov, Nikolay; Wouters, Johan; Collard, Laurent; Robiette, Raphaël; Berionni, Guillaume
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4772 - 4777
• a: 13.8967 ± 0.0008 Å
• b: 8.1179 ± 0.0003 Å
• c: 13.4003 ± 0.0007 Å
• α: 90°
• β: 113.349 ± 0.007°
• γ: 90°
• Cell volume: 1387.92 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.069
• Weighted residual factors for significantly intense reflections: 0.1533
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.359
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No