Information card for entry 7706911

Structure parameters

• Formula: C176 H288 Fe4 K4 N24 Si8
• Calculated formula: C176 H288 Fe4 K4 N24 Si8
• Title of publication: Quasilinear 3d-metal(i) complexes [KM(N(Dipp)SiR₃)₂] (M = Cr-Co) - structural diversity, solution state behaviour and reactivity.
• Authors of publication: Weller, Ruth; Müller, Igor; Duhayon, Carine; Sabo-Etienne, Sylviane; Bontemps, Sébastien; Werncke, C. Gunnar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4890 - 4903
• a: 20.857 ± 0.003 Å
• b: 13.086 ± 0.002 Å
• c: 19.863 ± 0.003 Å
• α: 90°
• β: 117.192 ± 0.01°
• γ: 90°
• Cell volume: 4822.1 ± 1.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0848
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1572
• Weighted residual factors for all reflections included in the refinement: 0.1679
• Goodness-of-fit parameter for all reflections included in the refinement: 0.938
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No