Information card for entry 7707095

Structure parameters

• Formula: C16 H61.5 Bi K6.17 N4 O96.67 P2 W22
• Calculated formula: C16 H48 Bi K6.16667 N4 O96.6666 P2 W22
• Title of publication: Keggin-type polyoxometalate 1 : 1 complexes of Pb(II) and Bi(III): experimental, theoretical and luminescence studies.
• Authors of publication: Mukhacheva, Anna A.; Asanova, Tatiana; Ryzhikov, Maxim R.; Sukhikh, Taisiya S.; Kompankov, Nikolay B.; Yanshole, Vadim V.; Berezin, Alexey S.; Gushchin, Artem L.; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 20
• Pages of publication: 6913 - 6922
• a: 48.525 ± 0.003 Å
• b: 12.692 ± 0.0008 Å
• c: 56.67 ± 0.003 Å
• α: 90°
• β: 109.593 ± 0.002°
• γ: 90°
• Cell volume: 32881 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0994
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1297
• Weighted residual factors for all reflections included in the refinement: 0.139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No