Information card for entry 7707577

Structure parameters

• Formula: C64 H96 Br4 K2 N2 O32 Ru8
• Calculated formula: C64 H96 Br4 K2 N2 O32 Ru8
• Title of publication: One-pot atmospheric pressure synthesis of [H₃Ru₄(CO)₁₂]<sup/>.
• Authors of publication: Cesari, Cristiana; Bortoluzzi, Marco; Femoni, Cristina; Iapalucci, Maria Carmela; Zacchini, Stefano
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 27
• Pages of publication: 9610 - 9622
• a: 14.0395 ± 0.0009 Å
• b: 16.7852 ± 0.0011 Å
• c: 21.5954 ± 0.0014 Å
• α: 74.768 ± 0.002°
• β: 72.962 ± 0.002°
• γ: 67.148 ± 0.002°
• Cell volume: 4419.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0819
• Residual factor for significantly intense reflections: 0.0696
• Weighted residual factors for significantly intense reflections: 0.1866
• Weighted residual factors for all reflections included in the refinement: 0.1918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No