Information card for entry 7707581

Structure parameters

• Formula: C39 H36 Br4 K0.5 N1.5 O33 Ru10
• Calculated formula: C39 H36 Br4 K0.5 N1.5 O33 Ru10
• Title of publication: One-pot atmospheric pressure synthesis of [H₃Ru₄(CO)₁₂]<sup/>.
• Authors of publication: Cesari, Cristiana; Bortoluzzi, Marco; Femoni, Cristina; Iapalucci, Maria Carmela; Zacchini, Stefano
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 27
• Pages of publication: 9610 - 9622
• a: 31.7547 ± 0.0015 Å
• b: 13.3024 ± 0.0006 Å
• c: 32.2056 ± 0.0015 Å
• α: 90°
• β: 99.623 ± 0.002°
• γ: 90°
• Cell volume: 13412.7 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.061
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1095
• Weighted residual factors for all reflections included in the refinement: 0.1128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.156
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No