Information card for entry 7707779
| Formula |
C29 H37 Al |
| Calculated formula |
C29 H37 Al |
| Title of publication |
Synthesis, structure and insertion reactivity of Lewis acidic 9-aluminafluorenes. |
| Authors of publication |
Drescher, Regina; Wüst, Leonie; Mihm, Cornelius; Krummenacher, Ivo; Hofmann, Alexander; Goettel, James; Braunschweig, Holger |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2021 |
| Journal volume |
50 |
| Journal issue |
30 |
| Pages of publication |
10400 - 10404 |
| a |
11.46 ± 0.003 Å |
| b |
13.928 ± 0.004 Å |
| c |
17.4 ± 0.004 Å |
| α |
105.12 ± 0.02° |
| β |
93.95 ± 0.02° |
| γ |
111.893 ± 0.012° |
| Cell volume |
2444.6 ± 1.2 Å3 |
| Cell temperature |
100 ± 2 K |
| Ambient diffraction temperature |
100 ± 2 K |
| Number of distinct elements |
3 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0665 |
| Residual factor for significantly intense reflections |
0.0497 |
| Weighted residual factors for significantly intense reflections |
0.1174 |
| Weighted residual factors for all reflections included in the refinement |
0.1257 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.045 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7707779.html
