Information card for entry 7708060

Structure parameters

• Formula: C21 H25 Al Li N3 O
• Calculated formula: C21 H25 Al Li N3 O
• Title of publication: Synthesis of tris(3-pyridyl)aluminate ligand and its unexpected stability against hydrolysis: revealing cooperativity effects in heterobimetallic pyridyl aluminates.
• Authors of publication: García-Romero, Álvaro; Martín-Álvarez, Jose M; Colebatch, Annie L.; Plajer, Alex J.; Miguel, Daniel; Álvarez, Celedonio M; García-Rodríguez, Raúl
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 37
• Pages of publication: 13059 - 13065
• a: 10.0339 ± 0.0008 Å
• b: 10.0431 ± 0.0006 Å
• c: 15.9941 ± 0.0012 Å
• α: 81.015 ± 0.006°
• β: 76.374 ± 0.007°
• γ: 60.358 ± 0.007°
• Cell volume: 1359.9 ± 0.2 ų
• Cell temperature: 220 ± 0.4 K
• Ambient diffraction temperature: 220 ± 0.4 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0847
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.2208
• Weighted residual factors for all reflections included in the refinement: 0.2392
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No