Information card for entry 7708183

Structure parameters

• Common name: WO_155
• Formula: C58 H100 B4 Li6 N6 O8
• Calculated formula: C58 H100 B4 Li6 N6 O8
• Title of publication: N-H deprotonation of a diaminodialkoxido diborane(4) - a structural study on bifunctional Lewis acids/bases and their dimerisation to B(sp²)₂B(sp³)₂N₂ six membered rings.
• Authors of publication: Drescher, Wiebke; Kleeberg, Christian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 37
• Pages of publication: 13149 - 13157
• a: 19.3963 ± 0.0012 Å
• b: 16.786 ± 0.0008 Å
• c: 22.9634 ± 0.0014 Å
• α: 90°
• β: 101.073 ± 0.006°
• γ: 90°
• Cell volume: 7337.4 ± 0.7 ų
• Cell temperature: 100.3 ± 0.2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0699
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.136
• Weighted residual factors for all reflections included in the refinement: 0.1497
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No