Information card for entry 7708196

Structure parameters

• Formula: C39 H45 N Si2
• Calculated formula: C39 H45 N Si2
• SMILES: [Si](N(c1c(cc(cc1C(c1ccccc1)c1ccccc1)C)C(c1ccccc1)c1ccccc1)[Si](C)(C)C)(C)(C)C
• Title of publication: On the edge of the steric repulsion and reactivity of bulky anilines; a case study of chloro(imino)phosphine synthesis
• Authors of publication: Vrána, Jan; Němec, Vlastimil; Samsonov, Maksim Andreevich; Růžička, Aleš
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 9.3294 ± 0.0005 Å
• b: 10.4494 ± 0.0006 Å
• c: 18.6129 ± 0.001 Å
• α: 78.955 ± 0.002°
• β: 84.572 ± 0.002°
• γ: 69.27 ± 0.002°
• Cell volume: 1664.89 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1455
• Residual factor for significantly intense reflections: 0.1341
• Weighted residual factors for significantly intense reflections: 0.3657
• Weighted residual factors for all reflections included in the refinement: 0.3715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No