Information card for entry 7708852

Structure parameters

• Formula: C37 H78 N4 P2 Si4 Sn2
• Calculated formula: C37 H78 N4 P2 Si4 Sn2
• SMILES: CC(C)[P]1(C(C)C)Cc2ccc(C(C)(C)c3ccc4C[P](C(C)C)(C(C)C)[Sn](n34)N([Si](C)(C)C)[Si](C)(C)C)n2[Sn]1N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Stannylenes based on pyrrole-phosphane and dipyrromethane-diphosphane scaffolds: syntheses and behavior as precursors to PSnP pincer palladium(II), palladium(0) and gold(I) complexes.
• Authors of publication: Cabeza, Javier A.; Fernández, Israel; García-Álvarez, Pablo; García-Soriano, Rubén; Laglera-Gándara, Carlos J; Toral, Rubén
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 44
• Pages of publication: 16122 - 16132
• a: 10.5334 ± 0.0009 Å
• b: 16.7794 ± 0.0015 Å
• c: 54.962 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9714.2 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1188
• Residual factor for significantly intense reflections: 0.0935
• Weighted residual factors for significantly intense reflections: 0.2245
• Weighted residual factors for all reflections included in the refinement: 0.243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No